HPLC Separation of Genotoxic Derivatives of Naphthalene

Authors

  • V. Quaiserova UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Charles University, Prague
  • J. Zima UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Charles University, Prague
  • J. Barek UNESCO Laboratory of Environmental Electrochemistry, Department of Analytical Chemistry, Charles University, Prague

Abstract

The following optimised conditions for the separation of naphthalene, naphthalen-1-amine, naphthalen-2-amine, 1- and 2-naphthols, and 1- and 2-nitronaphthalenes were found using a combination of the prediction of chromatographic behaviour of the tested substances with ChromSword® (Merck) optimisation software and experimental verification: LiChrospher® column, 24-min linear gradient, acetonitrile (40 - 70 %) - phosphate buffer, pH 2.3 (60 - 30 %), flow rate 0.5 ml/min, UV detection at 285 nm.

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Published

2000-12-15

How to Cite

Quaiserova, V., Zima, J., & Barek, J. (2000). HPLC Separation of Genotoxic Derivatives of Naphthalene. Chemické Listy, 94(11). Retrieved from http://blog.chemicke-listy.cz/ojs3/index.php/chemicke-listy/article/view/2473

Issue

Vol. 94 No. 11 (2000)

Section

Articles